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ASTM-D3278 2011

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D3278-96(2011) Standard Test Methods for Flash Point of Liquids by Small Scale Closed-Cup Apparatus

Published By Publication Date Number of Pages
ASTM 2011 8
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ASTM D3278-96-Reapproved2011

Historical Standard: Standard Test Methods for Flash Point of Liquids by Small Scale Closed-Cup Apparatus (Withdrawn 2020)

ASTM D3278

Scope

1.1 These test methods cover procedures for determining whether a material does or does not flash at a specified temperature or for determining the lowest finite temperature at which a material does flash when using a small scale closed-cup apparatus. The test methods are applicable to paints, enamels, lacquers, varnishes, and related products having a flash point between 0 and 110Ā°C (32 and 230Ā°F) and viscosity lower than 150 St at 25Ā°C (77Ā°F).

Note 1ā€”Tests at higher or lower temperatures are possible.

Note 2ā€”More viscous materials may be tested in accordance with Annex A4.

Note 3ā€”Organic peroxides may be tested in accordance with Annex A5, which describes the applicable safety precautions.

Note 4ā€”The U.S. Department of Labor (OSHA, Hazard Communications), the U.S. Department of Transportation (RSPA), and the U.S. Environmental Protection Agency (EPA) have specified Test Methods D3278 as one of several acceptable methods for the determination of flash point of liquids in their regulations.

Note 5ā€”These test methods are similar to International Standards ISO 3679 and ISO 3680.

1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.

1.3 This standard should be used to measure and describe the response of materials, products, or assemblies to heat and flame under controlled conditions and should not be used to describe or appraise the fire-hazard or fire-risk of materials, products, or assemblies under actual fire conditions. However, results of the test may be used as elements of a fire-hazard or a fire-risk assessment which takes into account all of the factors which are pertinent to an assessment of the fire hazard or fire risk of a particular end use.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see 8.1 and 11.2.

Keywords

flash/no flash; flash point; organic peroxides; organic solvents; small scale closed-cup apparatus; Butanol (sec/tert/n); Closed-cup flash point methods; Flash point–liquids; Lacquer; Organic peroxides; Setaflash testers; Varnishes; para-Xylene

ICS Code

ICS Number Code 13.220.40 (Ignitability and burning behaviour of materials and products)

DOI: 10.1520/D3278-96R11

PDF Catalog

PDF Pages PDF Title
1 Scope
Referenced Documents
Terminology
Summary of Test Methods
2 Significance and Use
Apparatus
Reagents and Materials
Sampling
Preparation of Apparatus
Procedureā€”Ambient to 110Ā°C (230Ā°F)
3 Procedureā€”0Ā°C (32Ā°F) to Ambient
Procedureā€”Ambient to 110Ā°C (230Ā°F)
Procedureā€”0Ā°C (32Ā°F) to Ambient Temperature
4 Clean-up of Apparatus and Preparation for Next Test
Correction for Barometric Pressure
Report
Precision and Bias
5 Keywords
A1. APPARATUS SPECIFICATIONS
A1.1
6 FIG. A1.1
7 A2. COOLING BLOCK
A2.1
A3. SPECIFICATIONS FOR p-XYLENE AND n-BUTANOL REFERENCE STANDARDS
A3.1 p-Xylene
A3.2 n-Butanol
FIG. A2.1
8 A4. TESTING HIGH VISCOSITY LIQUIDS
A4.1
A4.2
A5. TESTING ORGANIC PEROXIDES
A5.1
ASTM-D3278 2011
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