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ASTM-D3328 2000

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D3328-00 Standard Test Methods for Comparison of Waterborne Petroleum Oils by Gas Chromatography

Published By Publication Date Number of Pages
ASTM 2000 7
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1.1 This test method covers the comparison of petroleum oils recovered from water or beaches with oils from suspect sources by means of gas chromatography (1,2 ,3 ) . Such oils include distillate fuel, lubricating oil, and crude oil. The test method described is for capillary column analyses using either single detection (flame ionization) or dual detection (flame ionization and flame photometric) for sulfur containing species.

1.2 This test method provides high resolution for critical examination of fine structure that is resistant to weathering. The flame-photometric detection for sulfur components is an adjunct, not a substitute, for flame-ionization detection in the identification of waterborne petroleum oils (4-12) . For this reason, flame photometric detection is optional.

1.3 This standard does not purport to address the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

PDF Catalog

PDF Pages PDF Title
1 Scope
Referenced Documents
Terminology
Significance and Use
Interferences
2 Reagents and Materials
Reference Standards
Sampling
Summary of Test Method
Apparatus
3 Preparation of Chromatograph
Operating Conditions for Analysis (
)
TABLE 1
4 Component Identification
Procedure for a Sample
Interpretation
5 Report
Precision and Bias
Test Sample (Spilled oil)
Quality Assurance
Keywords
FIG. 1
6 A1. COLUMNS
A1.1 Column Performance
A1.2 Procedure
A1.3 Performance Standards
REFERENCES
ASTM-D3328 2000
$40.63