ASTM-D4628 2011

$40.63

D4628-05(2011)e1 Standard Test Method for Analysis of Barium, Calcium, Magnesium, and Zinc in Unused Lubricating Oils by Atomic Absorption Spectrometry

Published By	Publication Date	Number of Pages
ASTM	2011	7

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Categories: 71.040.50 - Physicochemical methods of analysis, ASTM

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Description

1.1 This test method is applicable for the determination of mass percent barium from 0.005 to 1.0 %, calcium and magnesium from 0.002 to 0.3 %, and zinc from 0.002 to 0.2 % in lubricating oils.

1.2 Higher concentrations can be determined by appropriate dilution. Lower concentrations of metals such as barium, calcium, magnesium, and zinc at about 10 ppm level can also be determined by this test method. Use of this test method for the determination at these lower concentrations should be by agreement between the buyer and the seller.

1.3 Lubricating oils that contain viscosity index improvers may give low results when calibrations are performed using standards that do not contain viscosity index improvers.

1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific warning statements are given in 3.1, 6.3, and 8.1.

PDF Catalog

PDF Pages	PDF Title
1	Scope Referenced Documents Summary of Test Method Significance and Use
2	Apparatus Reagents FIG. 1
3	Sampling Preparation of Apparatus Calibration (Barium) Procedure (Barium) Calculation (Barium)
4	Calcium Determination Magnesium Determination Zinc Determination Report Quality Control Precision and Bias Keywords TABLE 1
5	X1. QUALITY CONTROL MONITORING X1.1 X1.2 X1.3 X1.4 X1.5 X1.6 TABLE 2 TABLE 3
6	X2. HELPFUL HINTS FOR OPERATION OF THE TEST METHOD D4628 TEST X2.1 X2.2 X2.3 X2.4 X2.5 X2.6 X2.7 X2.8 X2.9 X2.10 X2.11 X2.12 X2.13 X2.14 X2.15 X2.16 X2.17 X2.18 X2.19 X2.20 X2.21 X2.22 X2.23 X2.24 X2.25
7	X2.26

Additional information

Standard Title	D4628-05(2011)e1 Standard Test Method for Analysis of Barium, Calcium, Magnesium, and Zinc in Unused Lubricating Oils by Atomic Absorption Spectrometry
Published Code	ASTM
Publication Date	2011
Pages Count	7
ICS Codes	71.040.50 - Physicochemical methods of analysis

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ASTM-D4628 2011

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