ASTM-D5464 2011

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D5464-11 Standard Test Method for pH Measurement of Water of Low Conductivity

Published By	Publication Date	Number of Pages
ASTM	2011	11

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Categories: 13.060.50 - Examination of water for chemical substances, ASTM

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Description

1.1 This test method is applicable to determine the pH of water samples with a conductivity of 2 to 100 ? S/cm over the pH range of 3 to 11. pH measurements of water of low conductivity are problematic. Specifically, this test method avoids contamination of the sample with atmospheric gases and prevents volatile components of the sample from escaping. This test method provides for pH electrodes and apparatus that address additional considerations discussed in Annex A2. This test method also minimizes problems associated with the sample’s pH temperature coefficient when the operator uses this test method to calibrate an on-line pH monitor or controller (see Appendix X1).

1.2 This test method covers the measurement of pH in water of low conductivity with a lower limit of 2.0 ? S/cm, utilizing a static grab-sample procedure where it is not practicable to take a real-time flowing sample.

Note 1Test Method D5128 for on-line measurement is preferred over this method whenever possible. Test Method D5128 is not subject to the limited conductivity range, temperature interferences, potential KCl contamination, and time limitations found with this method.

1.3 For on-line measurements in water with conductivity of 100 ? S/cm and higher, see Test Method D6569 .

1.4 For laboratory measurements in water with conductivity of 100 ? S/cm and higher, see Test Method D1193 .

1.5 The values stated in SI units are to be regarded as standard.

1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

PDF Catalog

PDF Pages	PDF Title
1	Scope Referenced Documents Terminology Reagents
2	Summary of Test Method Significance and Use Interferences
3	Apparatus Sampling and Sample Handling Calibration Procedure
4	Quality Control Precision and Bias Keywords FIG. 1
5	A1. DISCUSSION OF THE CONDUCTIVITY RANGE FOR THIS TEST METHOD A1.1 TABLE A1.1
6	A2. CONSIDERATIONS FOR THE REQUIREMENT OF SPECIALIZED pH MEASUREMENT APPARATUS A2.1 A2.2 TABLE A1.2
7	X1. TEMPERATURE EFFECTS IN PURE WATER X1.1 X1.2 X1.3 X1.4 TABLE X1.1
8	X1.5 X2. SUPPLEMENT FOR GRAB SAMPLE CALIBRATION (GSC) OF ON-LINE pH SENSORS X2.1 X2.2 X2.3 TABLE X1.2
9	X2.4 X2.5 X3. EFFECTS OF CO2 ON pH MEASUREMENTS OF HIGH PURITY WATER X3.1
10	FIG. X3.1
11	REFERENCES TABLE X3.1

Additional information

Standard Title	D5464-11 Standard Test Method for pH Measurement of Water of Low Conductivity
Published Code	ASTM
Publication Date	2011
Pages Count	11
ICS Codes	13.060.50 - Examination of water for chemical substances

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ASTM-D5464 2011

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