ASTM-D7035 2010

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D7035-10 Standard Test Method for Determination of Metals and Metalloids in Airborne Particulate Matter by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)

Published By	Publication Date	Number of Pages
ASTM	2010	28

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Categories: 13.040.20 - Ambient atmospheres, ASTM

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Description

1.1 This test method specifies a procedure for collection, sample preparation, and analysis of airborne particulate matter for the content of metals and metalloids using inductively coupled plasma-atomic emission spectrometry (ICP-AES).

1.2 The method is applicable to personal sampling of the inhalable or respirable fraction of airborne particles and to area sampling.

1.3 This test method should be used by analysts experienced in the use of ICP-AES, the interpretation of spectral and matrix interferences and procedures for their correction.

1.4 This method specifies a number of alternative methods for preparing test solutions from samples of airborne particulate matter. One of the specified sample preparation methods is applicable to the measurement of soluble metal or metalloid compounds. Other specified methods are applicable to the measurement of total metals and metalloids.

1.5 It is the user’s responsibility to ensure the validity of the standard method for filters of untested matrices.

1.6 The following is a non-exclusive list of metals and metalloids for which one or more of the sample dissolution methods specified in this document is applicable. However, there is insufficient information available on the effectiveness of dissolution methods for those elements in italics.

PDF Catalog

PDF Pages	PDF Title
1	Scope Referenced Documents
2	Terminology
4	Summary of Test Method
5	Significance and Use Sampling Apparatus and Materials Sampling Procedure
6	Hazards
7	Sample Preparation
8	Analysis
13	Expression of Results Method Performance
14	Records
15	Report Keywords A1. SAMPLE DISSOLUTION OF SOLUBLE METAL AND METALLOID COMPOUNDS A1.1 Overview A1.2 Effectiveness of the Sample Dissolution Method
16	A1.3 A1.4 A1.5 A1.6
17	A2. HOT PLATE DISSOLUTION OF METAL AND METALLOID COMPOUNDS A2.1 Overview
18	A2.2 Summary of Hot Plate Dissolution A2.3 Effectiveness of Hot Plate Dissolution Methods A2.4 A2.5
19	A2.6
20	A3. MICROWAVE DISSOLUTION OF METAL AND METALLOID COMPOUNDS A3.1 Overview A3.2 Summary of Microwave Dissolution Procedure A3.3 A3.4 A3.5
21	A3.6 Procedure
22	A4. HOT BLOCK DISSOLUTION OF METAL AND METALLOID COMPOUNDS ( A4.1 Overview A4.2 Summary of Hot Block Dissolution Procedure A4.3 Effectiveness of Hot Block Dissolution A4.4 A4.5 A4.6
23	X1. GUIDANCE ON FILTER SELECTION X1.1 Collection Efficiency X1.2 Dust-loading Capacity X1.3 Metal Content
24	X1.4 Weight Stability X1.5 Solubility X1.6 Chemical Compatibility X2. SPECIAL SAFETY PRECAUTIONS WHEN USING HYDROFLUORIC OR PERCHLORIC ACIDS X2.1 Special Precautions for use of Hydrofluoric Acid X2.2 Special Precautions for Use of Perchloric Acid
25	X3. GUIDANCE ON MAINTENANCE OF ICP-AES INSTRUMENTATION X3.1 Maintenance Contract X3.2 In-house Maintenance
26	X4. EXAMPLES OF PERFORMANCE CHECKS AND FAULT DIAGNOSTICS FOR ICP-AES X4.1 X4.2 X4.3 X4.4 X4.5 X4.6 X5. SAMPLER WALL DEPOSITS ( X5.1 X5.2 X5.3 X5.4
27	X5.5 X5.6 REFERENCES TABLE X5.1

Additional information

Standard Title	D7035-10 Standard Test Method for Determination of Metals and Metalloids in Airborne Particulate Matter by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
Published Code	ASTM
Publication Date	2010
Pages Count	28
ICS Codes	13.040.20 - Ambient atmospheres

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ASTM-D7035 2010

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