ASTM-E346 2008

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E346-08 Standard Test Method for Analysis of Methanol

Published By	Publication Date	Number of Pages
ASTM	2008	12

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Categories: 71.080.60 - Alcohols. Ethers, ASTM

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Description

1.1 These test methods cover chemical and physical tests for measuring the quality of methanol and appear in the following order:

1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.3 Review the current Material Safety Data Sheets (MSDS) for detailed information concerning toxicity, first aid procedures and safety precautions for the chemicals used in this standard.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific hazards statements are given in Sections 5 and 15 and in 16.1, 16.4, and 52.2.2.

10.1 This test method describes a procedure for detecting the presence of impurities in methanol that carbonize or darken in the presence of concentrated sulfuric acid. The test method is applicable to methanol having a carbonizables content in the range from 0 to 70 on the platinum-cobalt scale (see Test Method D 1209 ).

37.1 This test method is applicable to methanol in which the ethanol content is between 0 and 1000 ? g/g.

48.1 This test method covers a procedure for detecting the presence of acetone in methyl alcohol (methanol) in amounts greater than 0.003 weight % mass (m/m) .

56.1 This test method is used to determine the trimethylamine (TMA) content of refined methanol in the range of 10 to 100 ? g/kg.

56.2 The odor of methanol has been determined to be caused primarily by the impurity TMA. The determination of TMA and its relationship to odor will eliminate the need to sniff methanol to determined odor, avoiding exposure to this toxic chemical. Although TMA has been identified as the principal cause of odor, other compounds (amines, ethers) may contribute to odor.

PDF Catalog

PDF Pages	PDF Title
1	Scope Referenced Documents Significance and Use
2	Purity of Reagents Hazards Sampling Procedure Report Precision and Bias Scope Summary of Test Method Significance and Use TABLE 1
3	Apparatus Reagents Hazards Procedure Report Precision and Bias Procedure Report Precision and Bias TABLE 2
4	Procedure Report Precision and Bias Procedure Report Precision and Bias TABLE 3
5	Procedure Report Precision and Bias Procedure Report TABLE 4 TABLE 5
6	Precision and Bias Procedure Report Precision and Bias Scope Summary of Test Method Significance and Use Apparatus Reagents Preparation of Chromatographic Column
7	Calibration Procedure
8	Calculation Report Precision and Bias FIG. 1
9	Scope Summary of Test Method Significance and Use Apparatus Reagents Procedure Report Precision and Bias Scope TABLE 6
10	Summary of Test Method Significance and Use Apparatus Reagents and Materials Calibration and Standardization TABLE 7
11	Sample Analysis Procedure FIG. 2
12	Calculation Report Precision and Bias Keywords

Additional information

Safety Precautions	5
Acetone	48 to 55
Specific Gravity	28 to 30
Sampling	6
Permanganate Time	25 to 27
Purity of Reagents	4
Trimethylamine	56 to 65
Acidity	7 to 9
Color	19 to 21
Water Miscibility	34 to 37
Ethanol	37 to 47
Distillation Range	22 to 24
Carbonizables	10 to 18
Water	31 to 33
	Sections
ICS Codes	71.080.60 - Alcohols. Ethers

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ASTM-E346 2008

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