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BS EN 13639:2017

$142.49

Determination of total organic carbon in limestone

Published By Publication Date Number of Pages
BSI 2017 30
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This European Standard specifies methods for the determination of the total organic carbon content (TOC) in limestone. The standard describes the reference method and alternative methods which can be considered to be equivalent. In the case of a dispute, only the reference method is used. Any other methods may be used provided they are calibrated, either against the reference method or against internationally accepted reference materials, in order to demonstrate their equivalence.

PDF Catalog

PDF Pages PDF Title
2 National foreword
7 1 Scope
2 Normative references
3 General requirements for testing
3.1 Number of tests
3.2 General statistical terms
8 3.3 Expression of masses and results
3.4 Blank determinations
3.5 Sampling and sampling preparation
3.6 General test principles
9 4 Reagents
11 5 General apparatus
5.1 Balances
5.2 Laboratory ovens
12 5.3 Crucibles
6 Gravimetric method with wet oxidation (reference method)
6.1 Principle
6.2 Apparatus
13 6.3 Procedure
14 6.4 Calculation
7 Gravimetric method with furnace oxidation (alternative method No. 1)
7.1 Principle
7.2 Apparatus
16 7.3 Procedure
7.3.1 Filling the quartz tube
7.3.2 Preparing an absorption tube
7.3.3 Determination
7.4 Calculation
17 8 Infrared detection method with furnace oxidation (low temperature) (alternative method No. 2)
8.1 Principle
8.2 Apparatus
19 8.3 Procedure
8.3.1 Filling the quartz tube
8.3.2 Filling the absorption tower
8.3.3 Filling the adsorption tower
8.3.4 Adjustments
8.3.5 Cleaning
20 8.3.6 Calibration
8.3.7 Validation
8.3.8 Determination
8.4 Calculation
21 9 Infrared detection or conductivity methods with furnace oxidation (high temperature): procedure A (alternative method No. 3)
9.1 Principle
9.2 Apparatus
22 9.3 Procedure
9.3.1 Calibration
9.3.2 Determination
9.3.3 Expression of results
23 10 Infrared detection or conductivity methods with furnace oxidation (high temperature): procedure B (alternative method No. 4)
10.1 Principle
10.2 Apparatus
10.3 Procedure
10.3.1 Calibration
10.3.2 Determination
10.3.3 Expression of results
24 11 Repeatability and reproducibility standard deviation, determination limit
12 Test report
25 Annex A (informative)Features of commercial HF (High Frequency) combustion/infrared carbon analyzers
A.1 Combustion
26 A.2 Infrared gas analyser
27 Annex B (informative)Assignment of reagents to methods
BS EN 13639:2017
$142.49