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BS EN 16476:2014

$102.76

Liquid petroleum products. Determination of Sodium, Potassium, Calcium, Phosphorus, Copper and Zinc contents in diesel fuel. Method via Inductively Coupled Plasma Optical Emission Spectrometry (ICP OES)

Published By Publication Date Number of Pages
BSI 2014 18
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This European Standard specifies an inductively coupled plasma optical emission spectrometry (ICP OES) method for the determination of sodium, potassium, calcium, phosphorus, copper and zinc concentrations of diesel fuels, including those containing up to 30 % (V/V) fatty acid methyl ester (FAME), in the range detailed in Table 1. These six elements are considered as the most essential ash forming elements.

Table 1 Application ranges for ash forming elements

NOTE For the purposes of this European Standard, the term “% (V/V)” is used to represent the volume fraction, φ.

WARNING The use of this European Standard may involve hazardous materials, operations and equipment. This European Standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this European Standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

PDF Catalog

PDF Pages PDF Title
5 Foreword
6 Introduction
7 1 Scope
Table 1 — Application ranges for ash forming elements
2 Normative references
3 Principle
4 Reagents
8 5 Apparatus
9 Table 2 — Recommended wavelengths
10 6 Sampling
7 Preparation of calibration solutions
7.1 General
7.2 Internal Standard solution
7.3 Calibration solutions
Table 3 — Calibration solutions
11 7.4 Calibration check solution
Table 4 — Calibration check solution
8 Calibration
8.1 General
8.2 Calibration of the ICP OES spectrometer
12 8.3 Procedure A
8.4 Procedure B
8.5 Check of calibration
13 9 Sample analysis
9.1 Sample preparation
9.2 Sample measurement
14 10 Calculation
11 Expression of result
12 Precision
12.1 General
12.2 Repeatability
12.3 Reproducibility
15 Table 5 — Method precision
13 Test report
16 Bibliography
BS EN 16476:2014
$102.76