BS EN 16852:2017

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Foodstuffs. Determination of ethyl carbamate in stone fruit spirits, fruit marc spirits and other spirit drinks. GC-MS method

Published By	Publication Date	Number of Pages
BSI	2017	20

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Categories: 67.160.10 - Alcoholic beverages, BSI

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Description

This European Standard specifies a gas chromatographic method using mass spectrometric detection for the determination of ethyl carbamate (EC) in stone fruit spirits, fruit marc spirits and other spirit drinks. The method has been validated in an interlaboratory study for stone fruit spirits and fruit liqueurs, at levels ranging from 0,253 mg/l to 1,11 mg/l. However, linearity of the instrument response was proven for the concentration ranges 0,10 mg/l to 4,0 mg/l (simplified method) and 0,025 mg/l to 3,0 mg/l (procedure including sample clean-up), respectively.

PDF Catalog

PDF Pages	PDF Title
2	National foreword
6	1 Scope 2 Normative references 3 Principle 4 Reagents
9	5 Apparatus
10	6 Procedure 6.1 Preparation of samples for simplified method, dry extract < 10 g/l 6.2 Preparation of samples for method using sample clean up
11	7 Gas chromatography and mass spectrometry (GC-MS) 7.1 GC conditions 7.2 MS conditions 8 Calculation
12	9 Precision 9.1 General 9.2 Repeatability 9.3 Reproducibility
13	10 Test report
14	Annex A (informative)Typical chromatograms A.1 Using the simplified method, dry extract, < 10 g/l (see 6.1)
16	A.2 Using the method with sample clean up (see 6.2)
18	Annex B (informative)Precision data

Additional information

Status	Under Review
Pages	20
Publication Date	2017-08-04
ISBN	978 0 580 80859 3
Standard Number	BS EN 16852:2017
Title	Foodstuffs. Determination of ethyl carbamate in stone fruit spirits, fruit marc spirits and other spirit drinks. GC-MS method
Identical National Standard Of	EN 16852:2017
Descriptors	Spirit levels, Drinks, Food manufacturing processes, Food processes
Publisher	BSI
Committee	AW/275
ICS Codes	67.160.10 - Alcoholic beverages

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BS EN 16852:2017

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