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BS EN 17197:2023

BS EN 17197:2023

$189.07

Construction products: Assessment of release of dangerous substances. Analysis of inorganic substances in eluates and digests. Analysis by inductively coupled plasma optical emission spectrometry (ICP-OES)

Published By Publication Date Number of Pages
BSI 2023 48
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This document specifies the method for the determination of major, minor and trace elements in aqua regia and nitric acid digests and in eluates of construction products by inductively coupled plasma optical emission spectrometry (ICP-OES). It refers to the following 44 elements: Aluminium (Al), antimony (Sb), arsenic (As), barium (Ba), beryllium (Be), bismuth (Bi), boron (B), cadmium (Cd), calcium (Ca), cerium (Ce), chromium (Cr), cobalt (Co), copper (Cu), iron (Fe), lanthanum (La), lead (Pb), lithium (Li), magnesium (Mg), manganese (Mn), mercury (Hg), molybdenum (Mo), neodymium (Nd), nickel (Ni), phosphorus (P), potassium (K), praseodymium (Pr), samarium (Sm), scandium (Sc), selenium (Se), silicon (Si), silver (Ag), sodium (Na), strontium (Sr), sulphur (S), tellurium (Te), thallium (Tl), thorium (Th), tin (Sn), titanium (Ti), tungsten (W), uranium (U), vanadium (V), zinc (Zn), and zirconium (Zr). For the determination of low levels of As, Se and Sb, hydride generation can be applied. This method is described in Annex E. NOTE Construction products include e.g. mineral-based products (S); bituminous products (B); metals (M); wood-based products (W); plastics and rubbers (P); sealants and adhesives (A); paints and coatings (C), see also CEN/TR 16045. The method in this document is applicable to construction products and validated for the product types listed in Annex C.

PDF Catalog

PDF Pages PDF Title
2 undefined
8 1 Scope
2 Normative references
3 Terms and definitions
10 4 Abbreviations
11 5 Principle
6 Interferences
6.1 General
6.2 Spectral interferences
6.2.1 Background emission and stray light
12 6.2.2 Spectral overlaps
6.3 Non-spectral interferences
6.3.1 Physical interferences
6.3.2 Chemical interferences
6.3.3 Memory interferences
7 Reagents
14 8 Apparatus
15 9 Procedure
9.1 Test sample
9.2 Test portion
9.3 Instrument set up
9.3.1 General requirements
16 9.3.2 Inter-element correction
9.3.3 Internal standard
9.3.4 Instrument performance check
9.4 Calibration
9.4.1 Linear calibration function
17 9.4.2 Nonlinear calibration function
9.4.3 Standard addition calibration
9.5 Sample measurement
18 10 Calculation
10.1 Calculation for digests of construction products
10.2 Calculation for eluates of construction products
11 Expression of results
12 Performance characteristics
12.1 General
12.2 Blank
12.3 Calibration check
12.4 Interference
19 12.5 Recovery
12.6 Indicative values for MDL
13 Test performance
20 14 Test report
21 Annex A (informative)Wavelengths, spectral interferences and estimated method detection limits
25 Annex B (informative)Indicative values for MDL
26 Annex C (informative)Validation results for analysis of inorganic substances in digest and eluates from construction products
C.1 General
C.2 Precision data for analysis of eluates from construction products
33 C.3 Precision data for analysis of aqua regia digests from construction products
40 Annex D (informative)Inter element correction (IEC)
42 Annex E (normative)Determination of arsenic, antimony, mercury and selenium using chemical vapour generation ICP-OES
E.1 Scope
E.2 Principle
E.3 Apparatus
43 E.4 Reagents
44 E.5 Procedure
45 E.6 Calculation

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BS EN 17197:2023
$189.07