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BS EN ISO 11357-1:2023 – TC

BS EN ISO 11357-1:2023 – TC

$217.84

Tracked Changes. Plastics. Differential scanning calorimetry (DSC) – General principles

Published By Publication Date Number of Pages
BSI 2023 100
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PDF Catalog

PDF Pages PDF Title
1 30471266
57 A-30452381
58 undefined
60 European foreword
Endorsement notice
63 Foreword
64 Introduction
65 1 Scope
2 Normative references
3 Terms and definitions
72 4 Basic principles
4.1 General
4.2 Heat-flux DSC
4.3 Power-compensation DSC
73 5 Apparatus and materials
74 6 Specimen
75 7 Test conditions and specimen conditioning
7.1 Test conditions
7.2 Conditioning of specimens
8 Calibration
8.1 General
76 8.2 Calibration materials
8.3 Temperature calibration
8.3.1 General
8.3.2 Procedure
77 8.3.3 Accuracy of calibration
8.4 Heat calibration
8.4.1 General
78 8.4.2 Procedure
8.4.3 Accuracy of calibration
8.5 Heat flow rate calibration
8.5.1 General
79 8.5.2 Procedure
81 9 Procedure
9.1 Setting up the apparatus
9.1.1 Switching on
9.1.2 Purge gas
9.1.3 Experimental conditions
9.1.4 Baseline determination
9.2 Loading the specimen into the crucible
9.2.1 General
9.2.2 Selection of crucibles
82 9.2.3 Weighing the specimen crucible
9.2.4 Loading the specimen
9.2.5 Determination of the mass of the specimen
9.3 Insertion of crucibles into the instrument
9.4 Performing measurements
9.4.1 General
9.4.2 Scanning mode
83 9.4.3 Isothermal mode
84 9.5 Post-run checks
9.5.1 Check for loss in mass
9.5.2 Inspection of specimens
9.5.3 Checking of crucibles and crucible holder
10 Test report
86 Annex A (normative) Extended, high-precision, temperature calibration[12]
88 Annex B (normative) Extended, high-precision, heat calibration
90 Annex C (informative) Recommended calibration materials
94 Annex D (informative) Interaction of calibration materials with different crucible materials
96 Annex E (informative) General recommendations
98 Bibliography

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BS EN ISO 11357-1:2023 - TC
$217.84