BS EN ISO 9455-6:2022 – TC 2023
$186.33
Tracked Changes. Soft soldering fluxes. Test methods – Determination and detection of halide (excluding fluoride) content
Published By | Publication Date | Number of Pages |
BSI | 2023 | 54 |
This document specifies three quantitative methods for the determination of the ionic halide (excluding fluoride) content of soldering fluxes. Halides are calculated as chlorides. A useful qualitative test method for the detection of ionic halides is also described. Method A is a potentiometric titration method for the determination of halide (excluding fluoride) content and is applicable to flux classes 1 and 2, defined in ISO 9454-1. This method, which is considered the reference method for these fluxes, is suitable for halide contents generally within the range of 0,05 % mass fraction to 2 % mass fraction in the non-volatile matter of the flux. Method B is a titration method for the determination of the total halide (excluding fluoride) content of water-soluble fluxes. It is applicable to flux classes 2122 to 2124, 3112 to 3114 and 3212 to 3214, as defined in ISO 9454-1. Method C is a titration method for the determination of the halide (excluding fluoride) content of water-soluble fluxes containing phosphates and is applicable to flux class 331, as defined in ISO 9454-1. Method D is a qualitative test, using silver chromate test paper, for the presence of ionic halides. The technique can be used for all classes of flux.
PDF Catalog
PDF Pages | PDF Title |
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1 | 30468363 |
31 | A-30447671 |
32 | undefined |
34 | European foreword Endorsement notice |
36 | Foreword |
37 | 1 Scope 2 Normative references 3 Terms and definitions 4 Method A: Potentiometric method (Reference method) 4.1 Principle |
38 | 4.2 Reagents 4.3 Apparatus 4.4 Procedure |
39 | 4.5 Calculation of results 5 Method B: Titration method for halide (excluding fluoride) content of water-soluble fluxes 5.1 Principle |
40 | 5.2 Reagents 5.3 Apparatus 5.4 Procedure |
41 | 5.5 Standardization of the ammonium thiocyanate solution (5.2.2) 5.6 Calculation of results 6 Method C: Titration method for the determination of halide (excluding fluoride) content of water-soluble fluxes containing phosphates 6.1 Principle |
42 | 6.2 Reagents 6.3 Apparatus 6.4 Procedure |
43 | 6.5 Standardization of the ammonium thiocyanate solution (6.2.2) 6.6 Calculation of results 7 Method D: Qualitative test for the presence of ionic halides in flux 7.1 Principle 7.2 Reagents |
44 | 7.3 Apparatus 7.4 Procedure 7.4.1 Preparation of flux test solution |
45 | 7.4.2 Test procedure 8 Precision 8.1 General |
46 | 8.2 Method A 8.3 Method B 8.4 Method C 9 Test report |
48 | Annex A (normative) Method for standardizing the silver nitrate solution |
51 | Bibliography |