BS ISO 22863-9:2021
$102.76
Fireworks. Test methods for determination of specific chemical substances – Mercury content by hydride generation atomic fluorescence spectrometry
Published By | Publication Date | Number of Pages |
BSI | 2021 | 18 |
This document specifies the test method for the determination of the mercury content in pyrotechnic compositions by hydride generation atomic fluorescence spectrometry.
PDF Catalog
PDF Pages | PDF Title |
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2 | National foreword |
6 | Foreword |
9 | 1 Scope 2 Normative references 3 Terms and definitions 4 Principle of the method 5 Reagents 5.1 Hydrochloric acid (GR) 5.2 Nitric acid (GR) 5.3 Potassium dichromate (GR) |
10 | 5.4 Sodium hydroxide (GR) 5.5 Potassium borohydride (AR) 5.6 Nitric acid solution (volume fraction 5 %): 5.7 Nitric diluted solution of potassium dichromate (0,5 g/l): 5.8 Hydrochloric acid-nitric acid mixed reagent [(1 + 1) aqua regia]: 5.9 Sodium hydroxide solution (mass fraction 0,2 %): 5.10 Potassium borohydride solution (mass fraction 2 %): 5.11 Mercury standard solution (1 000 mg/l) 5.12 Mercury standard intermediate solution (1 µg/ml): 5.13 Mercury standard use solution (20 µg/l): 5.14 Preparation of mercury standard working curve solutions: 6 Apparatus 6.1 Agate mortar 6.2 80 mesh standard sample sieve 6.3 Water bath |
11 | 6.5 Volumetric flasks (50 ml) 6.7 Filter paper 7 Test procedure 7.1 Sample pre-treatment, digestion and preparation of the solution to be tested 7.2 Test conditions 8 Calculations |
12 | 9 Accuracy 10 Other 11 Test report |
13 | Annex A (informative) Standard addition method |