BSI 23/30435297 DC 2023
$13.70
BS ISO 6323-1. Workplace air. Determination of arsenic and arsenic compounds by electrothermal atomic absorption spectrometry – Part 1. Arsenic and arsenic compounds, except arsine by ET-AAS
Published By | Publication Date | Number of Pages |
BSI | 2023 | 30 |
PDF Catalog
PDF Pages | PDF Title |
---|---|
7 | Foreword |
8 | Introduction |
9 | 1 Scope 2 Normative references 3 Terms and definitions |
10 | 4 Principle 5 Requirement 6 Apparatus and equipment 6.1 Sampling equipment 6.1.1 Sampler |
11 | 6.1.2 Filter capsule 6.1.3 Sampling pumps 6.1.4 Portable flowmeter 6.1.5 Silicone adapter 6.1.6 Ancillary equipment 6.2 Collection media 6.2.1 Filters |
12 | 6.2.2 Requirements for filters |
13 | 6.2.3 Back pressure of filters 6.2.4 Weighing of filters 6.3 Equipment for the determination of dust concentration 6.4 Equipment for sample digestion 6.4.1 General 6.4.2 Equipment for all types of sample digestion 6.4.3 Laboratory equipment for open vessel hot block digestion |
14 | 6.4.4 Laboratory equipment for high pressure microwave digestion 6.5 Equipment for analysis 6.5.1 General 6.5.2 Equipment for sample preparation 6.5.3 Analytical system 7 Reagents 7.1 General |
15 | 7.2 Water 7.3 Chemicals for digestion 7.4 Chemicals for analysis 7.4.1 Stabilization and modifier 7.4.2 Calibration and quality control standards 7.5 Chemicals for method validation 8 Occupational exposure assessment |
16 | 9 Sampling 9.1 Preliminary considerations 9.1.1 Collection characteristics and flow rate 9.1.2 Sampling period 9.1.3 Temperature and pressure effects |
17 | 9.1.4 Sample handling 9.2 Sample preparation 9.2.1 Cleaning 9.2.2 Filter 9.2.3 Marking 9.2.4 Pre-weighing of filters 9.2.5 Assembly 9.3 Sampling preparation 9.3.1 Initial flow rate 9.3.2 Field blanks |
18 | 9.3.3 Personal sampling 9.3.4 Static sampling 9.4 Parameters 9.5 Performing the sampling 9.5.1 Start |
19 | 9.5.2 Sampling period 9.5.3 End 9.6 Transport and storage 9.6.1 Transportation 9.6.2 Storage |
20 | 10 Analysis 10.1 Preparation 10.1.1 General 10.1.2 Weighing 10.1.3 Digestion |
21 | 10.1.4 Solutions 10.2 Instrumental analysis |
22 | 10.3 Estimation of detection and quantification limits 10.3.1 Estimation of the instrumental detection limit |
23 | 10.3.2 Estimation of the method detection limit and quantification limit 10.4 Certified reference materials 10.5 Measurement uncertainty |
24 | 11 Expression of results 11.1 Calculations 11.2 Method performance 11.3 Remarks |
25 | 12 Test report 12.1 Test record |
26 | 12.2 Laboratory report |
27 | Annex€A (informative) Temperature and pressure correction |
29 | Annex€B (informative) Typical operating parameters for determination of arsenic by electrothermal atomic absorption spectrometry |
30 | Bibliography |