DIN EN 17322:2021 Edition

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Environmental Solid Matrices – Determination of polychlorinated biphenyls (PCB) by gas chromatography – mass selective detection (GC-MS) or electron-capture detection (GC-ECD)

Published By	Publication Date	Number of Pages
DIN	2021-03	51

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Categories: 13.030.01 - Wastes in general, 13.030.10 - Solid wastes, 13.030.20 - Liquid wastes. Sludge, 13.080.10 - Chemical characteristics of soils, DIN

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Description

This document specifies a method for quantitative determination of seven selected polychlorinated biphenyls (PCB28, PCB52, PCB101, PCB118, PCB138, PCB153 and PCB180) in environmental solid matrices using using high-resolution gas chromatography with electron capture or mass spectrometric detection. The limit of detection depends on the determinants, the equipment used, the quality of chemicals used for the extraction of the sample and the clean-up of the extract. Under the conditions specified in this European Standard draft, lower limit of application from 1 µg/kg (expressed as dry matter) for soils, sludge and biowaste to 10 µg/kg (expressed as dry matter) for solid waste can be achieved. For some specific samples the limit of 10 µg/kg cannot be reached. Sludge, waste and treated biowaste may differ in properties, as well as in the expected contamination levels of PCBs and presence of interfering substances. These differences make it impossible to describe one general procedure. This draft European standard contains decision tables based on the properties of the sample and the extraction and clean-up procedure to be used. The method may be applied to the analysis of other PCB congeners not specified in the scope, provided suitability is proven by proper in-house validation experiments

Additional information

Published Code	DIN
Published By	Deutsches Institut für Normung
Publication Date	2021-03
Pages Count	51
Language	Germany
Descriptors	Bio-wastes, Biphenyl, Characterisations, Chemical analysis and testing, Chemical elements, Chlorine, Compost, Definitions, Derivatives, Determination of content, Detrimental to health, Electron capture detectors, Elements, Gas chromatography, Health hazards, Injury to health, Inter-laboratory tests, Mass concentration, Mass spectrometry, Mathematical calculations, Methods of analysis, PCB, Photometry (chemical analysis), Polychlorinated biphenyls, Sampling methods, Sewage sludge, Sludge, Soil surveys, Soils, Solids, Testing, Trace elements, Waste disposal, Waste handling, Wastes, Water practice, Bottom, Ring tests, Ground, Floors, Gas phase chromatography
File Size	1.7 MB
ICS Codes	13.030.01 - Wastes in general 13.030.10 - Solid wastes 13.030.20 - Liquid wastes. Sludge 13.080.10 - Chemical characteristics of soils

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DIN EN 17322:2021 Edition

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