{"id":319225,"date":"2024-10-19T22:03:37","date_gmt":"2024-10-19T22:03:37","guid":{"rendered":"https:\/\/pdfstandards.shop\/product\/uncategorized\/bs-en-iso-787-282020\/"},"modified":"2024-10-25T20:22:11","modified_gmt":"2024-10-25T20:22:11","slug":"bs-en-iso-787-282020","status":"publish","type":"product","link":"https:\/\/pdfstandards.shop\/product\/publishers\/bsi\/bs-en-iso-787-282020\/","title":{"rendered":"BS EN ISO 787-28:2020"},"content":{"rendered":"
This document specifies a method for determining the total content of polychlorinated biphenyls (PCBs), checking for all 209 possible congeners in pigment materials.<\/p>\n
This document is applicable to a working range from1 mg\/kg to 150 mg\/kg. The lower quantitation limit of this method is 1 mg\/kg per congener. Results below 1 mg\/kg are considered to be qualitative only.<\/p>\n
PDF Pages<\/th>\n | PDF Title<\/th>\n<\/tr>\n | ||||||
---|---|---|---|---|---|---|---|
2<\/td>\n | National foreword <\/td>\n<\/tr>\n | ||||||
4<\/td>\n | European foreword <\/td>\n<\/tr>\n | ||||||
6<\/td>\n | Foreword <\/td>\n<\/tr>\n | ||||||
7<\/td>\n | Introduction <\/td>\n<\/tr>\n | ||||||
9<\/td>\n | 1 Scope 2 Normative references 3 Terms and definitions <\/td>\n<\/tr>\n | ||||||
10<\/td>\n | 4 Principle 5 Sampling 6 Procedure 6.1 General <\/td>\n<\/tr>\n | ||||||
11<\/td>\n | 6.2 Clean-up to eliminate interfering species 6.3 Separation and quantification 7 Reagents 7.1 Safety precautions <\/td>\n<\/tr>\n | ||||||
12<\/td>\n | 7.2 Reagents, solvents and absorbents 7.3 Internal reference materials for PCBs, 13C12-labelled <\/td>\n<\/tr>\n | ||||||
13<\/td>\n | 7.4 Cleaning\/disposal agents 8 Apparatus <\/td>\n<\/tr>\n | ||||||
14<\/td>\n | 9 Procedure 9.1 Preparation of test sample <\/td>\n<\/tr>\n | ||||||
15<\/td>\n | 9.2 Liquid-liquid extraction 9.2.1 Separation funnel <\/td>\n<\/tr>\n | ||||||
16<\/td>\n | 9.2.2 Ludwig extraction 9.3 Clean-up 9.3.1 General 9.3.2 Diatomaceous earth-sulfuric acid column (optional) <\/td>\n<\/tr>\n | ||||||
17<\/td>\n | 9.3.3 Gel permeation (size exclusion) chromatography\/porous styrene divinylbenzene beads-column (optional) <\/td>\n<\/tr>\n | ||||||
18<\/td>\n | 9.3.4 Multilayer columns (obligatory) <\/td>\n<\/tr>\n | ||||||
19<\/td>\n | 9.3.5 Alumina column (optional) 9.4 Preparation of GC solution and GC procedure <\/td>\n<\/tr>\n | ||||||
20<\/td>\n | 9.5 Calculation and quantitation procedure <\/td>\n<\/tr>\n | ||||||
21<\/td>\n | 10 Test report <\/td>\n<\/tr>\n | ||||||
23<\/td>\n | Annex A (informative) Nomenclature of PCBs <\/td>\n<\/tr>\n | ||||||
29<\/td>\n | Bibliography <\/td>\n<\/tr>\n<\/table>\n","protected":false},"excerpt":{"rendered":" General methods of tests for pigments and extenders – Determination of total content of polychlorinated biphenyls (PCB) by dissolution, cleanup and GC-MS<\/b><\/p>\n |