{"id":364072,"date":"2024-10-20T01:48:54","date_gmt":"2024-10-20T01:48:54","guid":{"rendered":"https:\/\/pdfstandards.shop\/product\/uncategorized\/bs-en-15199-22020\/"},"modified":"2024-10-26T02:51:53","modified_gmt":"2024-10-26T02:51:53","slug":"bs-en-15199-22020","status":"publish","type":"product","link":"https:\/\/pdfstandards.shop\/product\/publishers\/bsi\/bs-en-15199-22020\/","title":{"rendered":"BS EN 15199-2:2020"},"content":{"rendered":"

This document specifies a method for the determination of the boiling range distribution of petroleum products by capillary gas chromatography using flame ionization detection. The standard is applicable to materials having a vapour pressure low enough to permit sampling at ambient temperature, and which have a boiling range of at least 100 \u00b0C. The standard is applicable to materials with initial boiling points (IBP) above 100 \u00b0C and final boiling points (FBP) above 750 \u00b0C, for example, heavy distillate fuels and residuals. The method is not applicable to bituminous samples.<\/p>\n

The test method is not applicable for the analysis of petroleum or petroleum products containing low molecular weight components (for example naphthas, reformates, gasolines) or middle distillates like Diesel and Jet fuel.<\/p>\n

Petroleum or petroleum products containing blending components, which contain hetero atoms (for example alcohols, ethers, acids, or esters) or residue, are not to be analysed by this test method.<\/p>\n

\n
\n NOTE\n <\/div>\n

For the purposes of this document, the terms \u201c% ( m\/m<\/i>)\u201d and \u201c% ( V\/V<\/i>)\u201d are used to represent respectively the mass fraction and the volume fraction.<\/p>\n<\/div>\n

\n
\n WARNING\n <\/div>\n

The use of this document may involve hazardous materials, operations and equipment. This document does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and to determine the applicability of regulatory limitations prior to use.<\/p>\n<\/div>\n

PDF Catalog<\/h4>\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n
PDF Pages<\/th>\nPDF Title<\/th>\n<\/tr>\n
2<\/td>\nundefined <\/td>\n<\/tr>\n
6<\/td>\n1 Scope
2 Normative references
3 Terms and definitions <\/td>\n<\/tr>\n
8<\/td>\n4 Principle
5 Reagents and materials <\/td>\n<\/tr>\n
11<\/td>\n6 Apparatus <\/td>\n<\/tr>\n
13<\/td>\n7 Sampling
8 Preparation of the apparatus
8.1 Gas chromatograph preparation
8.2 System performance check
9 Sample and reference material preparation <\/td>\n<\/tr>\n
14<\/td>\n10 Calibration <\/td>\n<\/tr>\n
16<\/td>\n11 Procedure <\/td>\n<\/tr>\n
17<\/td>\n12 Visual inspection of the chromatograms
13 Calculation
14 Expression of results
15 Precision
15.1 General
15.2 Repeatability
15.3 Reproducibility <\/td>\n<\/tr>\n
19<\/td>\n16 Test report <\/td>\n<\/tr>\n
20<\/td>\nAnnex A (normative)Calculation procedure
A.1 Application
A.2 Starting conditions
A.3 Zero sample or reference chromatogram
A.4 Sample area
A.5 Start of sample elution time <\/td>\n<\/tr>\n
21<\/td>\nA.6 End of sample elution time
A.7 End of reference material elution time
A.8 Corrected sample or reference material area
A.9 Normalization
A.10 Conversion of retention time to percent off
A.10.1 Initial boiling point <\/td>\n<\/tr>\n
22<\/td>\nA.10.2 Intermediate boiling points
A.11 Conversion of retention times to boiling points <\/td>\n<\/tr>\n
23<\/td>\nAnnex B (normative)System performance check
B.1 Frequency
B.2 Column resolution
B.3 Detector response (gravimetric blend) <\/td>\n<\/tr>\n
24<\/td>\nB.4 Skewing of peak <\/td>\n<\/tr>\n
25<\/td>\nAnnex C (normative)Boiling points of n-alkanes <\/td>\n<\/tr>\n
27<\/td>\nAnnex D (informative)Additional guidance for the calculation algorithm
D.1 Zeroing of the reference material chromatogram
D.2 Zeroing of sample chromatograms <\/td>\n<\/tr>\n
28<\/td>\nD.3 Blank baseline subtraction from the sample chromatogram
D.4 Quenching correction
D.5 Determination of the sample final elution time (tFE)
D.6 Determination of the sample area
D.7 Response factor <\/td>\n<\/tr>\n
29<\/td>\nD.8 Calculation of the percentage recovery <\/td>\n<\/tr>\n
30<\/td>\nD.9 Determination of the boiling point distribution
D.10 Calculation of cut point intervals <\/td>\n<\/tr>\n<\/table>\n","protected":false},"excerpt":{"rendered":"

Petroleum products. Determination of boiling range distribution by gas chromatography method – Heavy distillates and residual fuels<\/b><\/p>\n\n\n\n\n
Published By<\/td>\nPublication Date<\/td>\nNumber of Pages<\/td>\n<\/tr>\n
BSI<\/b><\/a><\/td>\n2021<\/td>\n32<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n","protected":false},"featured_media":364081,"template":"","meta":{"rank_math_lock_modified_date":false,"ep_exclude_from_search":false},"product_cat":[2641],"product_tag":[],"class_list":{"0":"post-364072","1":"product","2":"type-product","3":"status-publish","4":"has-post-thumbnail","6":"product_cat-bsi","8":"first","9":"instock","10":"sold-individually","11":"shipping-taxable","12":"purchasable","13":"product-type-simple"},"_links":{"self":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product\/364072","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product"}],"about":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/types\/product"}],"wp:featuredmedia":[{"embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/media\/364081"}],"wp:attachment":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/media?parent=364072"}],"wp:term":[{"taxonomy":"product_cat","embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product_cat?post=364072"},{"taxonomy":"product_tag","embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product_tag?post=364072"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}