ASTM-C761:2004 Edition

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C761-04e1 Standard Test Methods for Chemical, Mass Spectrometric, Spectrochemical, Nuclear, and Radiochemical Analysis of Uranium Hexafluoride

Published By	Publication Date	Number of Pages
ASTM	2004	36

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Categories: 27.120.30 - Fissile materials and nuclear fuel technology, ASTM

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Description

1.1 These test methods cover procedures for subsampling and for chemical, mass spectrometric, spectrochemical, nuclear, and radiochemical analysis of uranium hexafluoride UF ₆ . Most of these test methods are in routine use to determine conformance to UF ₆ specifications in the Enrichment and Conversion Facilities.

1.2 The analytical procedures in this document appear in the following order:

Note 1Subcommittee C26.05 will confer with C26.02 concerning the renumbered section in Test Methods C761 to determine how concerns with renumbering these sections, as analytical methods are replaced with stand-alone analytical methods, are best addressed in subsequent publications.

1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. (For specific safeguard and safety consideration statements, see Section 6.)

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PDF Pages	PDF Title
1	Scope Referenced Documents
2	Significance and Use Reagents Rejection Safety Considerations
3	Scope Summary of Test Method Apparatus
4	Procedure FIG. 1 FIG. 2
5	FIG. 3 FIG. 4
7	Scope Summary of Test Method Interferences Apparatus Reagents Sampling Procedure FIG. 5
8	Calculation Precision and Bias Scope Scope
9	Scope Scope Summary of Test Method Apparatus TABLE 3
10	Procedure TABLE 4
11	Calculation
12	Reliability Scope Summary of Test Method Interferences Apparatus Procedure
13	Calculation Reliability Scope Scope Scope Summary of Test Method Apparatus Reagents
14	Procedure Calculation Reliability Scope Summary of Test Method FIG. 6
15	Interferences Apparatus Reagents Procedure
16	Reliability Scope Summary of Test Method Limitations Apparatus
17	Reagents Procedure FIG. 7
18	Photometry and Calculation Reliability Scope Scope Scope Scope Scope Summary of Test Method Apparatus Reagents
19	Procedure Reliability Scope Scope FIG. 8
20	Summary of Test Method Apparatus Reagents Procedure
21	Reliability Scope Scope Scope Scope TABLE 5
22	Summary of Test Method Apparatus Reagents Procedure FIG. 9
23	Calculation Reliability Scope Scope Summary of Test Method
24	Apparatus Reagents Procedure Scope Summary of Test Method
25	Interferences Apparatus Reagents Procedure Calculations Reliability
26	Scope Summary of Test Method Interferences Apparatus Reagents Procedure
27	Calculations Reliability Scope Summary of Test Method Interferences Apparatus Reagents Procedure
28	Precision and Bias Scope Summary of Test Method Interferences Apparatus Reagents Procedure
29	Precision and Bias Scope Summary of Test Method Apparatus Reagents Procedure
30	Counting Calculations Precision and Bias Sensitivity Scope Scope
31	Summary of Test Method Interferences Instrumentation and Apparatus Reagents Preparation of Apparatus Calibration Procedure TABLE 6
32	Calculation Precision and Bias Scope Summary of Test Method TABLE 7 TABLE 8
33	Interferences Instrumentation and Apparatus Reagents Preparation of Apparatus Calibration and Standardization TABLE 9 TABLE 10
34	Procedure Calculation Precision and Bias Keywords X1. LIST OF ALTERNATIVE STAND ALONE ASTM TEST METHODS TABLE 11
35	REFERENCES

Additional information

Determination of Uranium-232 by Alpha Spectrometry	80-86
Determination of Plutonium by Extraction and Alpha Counting	93-100
Isotopic Analysis by Double-Standard Mass-Spectrometer Method	23 – 29
Subsampling of Uranium Hexafluoride	7 – 10
Determination of Hydrocarbons, Chlorocarbons, and Partially Substituted Halohydrocarbons	29-36
Determination of Boron-Equivalent Neutron Cross Section	78
Titrimetric Determination of Chlorine	38-44
Isotopic Analysis	22
Determination of Tungsten	63
Preparation of High-Purity U 3 O 8	21
Determination of Titanium and Vanadium	61
Determination of Thorium and Rare Earths	64-69
Atomic Absorption Determination of Metallic Impurities	71-76
Atomic Absorption Determination of Chromium Insoluble In Uranium Hexafluoride	116-122
Determination of Uranium-233 Abundance by Thermal Ionization Mass Spectrometry	79
Determination of Plutonium by Ion Exchange and Alpha Counting	88-92
Atomic Absorption Determination of Chromium Soluble In Uranium Hexafluoride	109-115
Determination of Silicon and Phosphorus	45-51
Determination of Ruthenium	60
Determination of Molybdenum, Niobium, Tantalum, Titanium, and Tungsten by ICP-AES	143-152
Spectrophotometric Determination of Bromine	37
Determination of Technetium-99 In Uranium Hexafluoride	123-131
Determination of Fission Product Activity	87
Gravimetric Determination of Uranium	11 – 19
Determination of Molybdenum	70
Method for the Determiation of Gamma-Energy Emission Rate from Fission Products in Uranium Hexafluoride	132
Titrimetric Determination of Uranium	20
Atomic Absorption Determination of Antimony	36
Determination of Boron and Silicon	52-59
Determination of Neptunium by Extraction and Alpha Counting	101-108
Spectrographic Determination of Metallic Impurities	62
Determination of Metallic Impurities by ICP-AES	133-142
Impurity Determination by Spark-Source Mass Spectrography	77
ICS Codes	27.120.30 - Fissile materials and nuclear fuel technology
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