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BSI PD CEN/TS 17200:2018

$142.49

Construction products. Assessment of release of dangerous substances. Analysis of inorganic substances in digests and eluates. Analysis by Inductively Coupled Plasma. Mass Spectrometry (ICP-MS)

Published By Publication Date Number of Pages
BSI 2018 30
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This Technical Specification specifies the method for the determination of major, minor and trace elements in aqua regia and nitric acid digests and in eluates of construction products by Inductively Coupled Plasma – Mass Spectrometry (ICP-MS). It refers to the following 67 elements: Aluminium (Al), antimony (Sb), arsenic (As), barium (Ba), beryllium (Be), bismuth (Bi), boron (B), cadmium (Cd), calcium (Ca), cerium (Ce), cesium (Cs), chromium (Cr), cobalt (Co), copper (Cu), dysprosium (Dy), erbium (Er), europium (Eu), gadolinium (Gd), gallium (Ga), germanium (Ge), gold (Au), hafnium (Hf), holmium (Ho), indium (In), iridium (Ir), iron (Fe), lanthanum (La), lead (Pb), lithium (Li), lutetium (Lu), magnesium (Mg), manganese (Mn), mercury (Hg), molybdenum (Mo), neodymium (Nd), nickel (Ni), palladium (Pd), phosphorus (P), platinum (Pt), potassium (K), praseodymium (Pr), rubidium (Rb), rhenium (Re), rhodium (Rh), ruthenium (Ru), samarium (Sm), scandium (Sc), selenium (Se), silicon (Si), silver (Ag), sodium (Na), strontium (Sr), sulphur (S), tellurium (Te), terbium (Tb), thallium (Tl), thorium (Th), thulium (Tm), tin (Sn), titanium (Ti), tungsten (W), uranium (U), vanadium (V), ytterbium (Yb), yttrium (Y), zinc (Zn), and zirconium (Zr). NOTE 1 Construction products include e.g. mineral-based products (S); bituminous products (B); metals (M); wood-based products (W); plastics and rubbers (P); sealants and adhesives (A); paints and coatings (C), see also CEN/TR 16045 [1]. The working range depends on the matrix and the interferences encountered. NOTE 2 The limit of detection of most elements will be affected by their natural abundance, ionization behaviour, on abundance of isotope(s) free from isobaric interferences and by contamination (e.g. handling and airborne). Handling contaminations are in many cases more important than airborne ones. The limit of detection will be higher in cases where the determination is likely to be interfered (see Clause 4) or in case of memory effects (see e.g. EN ISO 17294-1:2006, 8.2). The method in this Technical Specification is applicable to construction products and validated for the product types listed in Annex B.

PDF Catalog

PDF Pages PDF Title
2 undefined
8 1 Scope
2 Normative references
9 3 Terms and definitions
11 4 Symbols and abbreviations
5 Principle
6 Interferences
6.1 General
6.2 Spectral interferences
6.2.1 Isobaric elemental interferences
12 6.2.2 Isobaric molecular and doubly charged ion interferences
6.3 Non spectral interferences
7 Reagents
15 8 Apparatus
16 9 Procedure
9.1 Test sample
9.2 Test portion
9.3 Instrument set up
17 9.4 Calibration
9.4.1 Calibration function
9.4.2 Standard addition calibration
18 9.4.3 Determination of correction factors
9.4.4 Variable isotope ratio
9.5 Sample measurement
10 Calculation
10.1 Calculation for digests of construction products
19 10.2 Calculation for eluates of construction products
11 Expression of results
12 Performance characteristics
12.1 General
12.2 Blank
12.3 Calibration check
12.4 Internal standard response
12.5 Interference
12.6 Recovery
12.7 Precision
20 13 Test report
22 Annex A (informative)Method detection limit (MDL) and precision data for soil, sludge and biowaste
30 Annex B (informative)Validation results for construction products
B.1 Introduction
B.2 Performance data
BSI PD CEN/TS 17200:2018
$142.49