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ASTM-C1165:2012 Edition

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C1165-12 Standard Test Method for Determining Plutonium by Controlled-Potential Coulometry in H2SO4 at a Platinum Working Electrode

Published By Publication Date Number of Pages
ASTM 2012 6
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1.1 This test method covers the determination of milligram quantities of plutonium in unirradiated uranium-plutonium mixed oxide having a U/Pu ratio range of 0.1 to 10. This test method is also applicable to plutonium metal, plutonium oxide, uranium-plutonium mixed carbide, various plutonium compounds including fluoride and chloride salts, and plutonium solutions.

1.2 The recommended amount of plutonium for each aliquant in the coulometric analysis is 5 to 10 mg. Precision worsens for lower amounts of plutonium, and elapsed time of electrolysis becomes impractical for higher amounts of plutonium.

1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 8.

PDF Catalog

PDF Pages PDF Title
1 Scope
Referenced Documents
Summary of Test Method
2 Significance and Use
Interferences
FIG. 1
3 Apparatus
Reagents
Safety Precautions
4 Preparation of Apparatus
Calibration
Procedure
5 Calculation of Sample Result
Precision and Bias
Keywords
REFERENCES
ASTM-C1165
$40.63