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ASTM-D6304 2007

$40.63

D6304-07 Standard Test Method for Determination of Water in Petroleum Products, Lubricating Oils, and Additives by Coulometric Karl Fischer Titration

Published By Publication Date Number of Pages
ASTM 2007 6
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1.1 This test method covers the direct determination of water in the range of 10 to 25 000 mg/kg entrained water in petroleum products and hydrocarbons using automated instrumentation. This test method also covers the indirect analysis of water thermally removed from samples and swept with dry inert gas into the Karl Fischer titration cell. Mercaptan, sulfide (S or H 2 S), sulfur, and other compounds are known to interfere with this test method (see Section 5).

1.2 This test method is intended for use with commercially available coulometric Karl Fischer reagents and for the determination of water in additives, lube oils, base oils, automatic transmission fluids, hydrocarbon solvents, and other petroleum products. By proper choice of the sample size, this test method may be used for the determination of water from mg/kg to percent level concentrations.

1.3 The values stated in SI units are to be regarded as standard. No other units of measurements are included in this standard.

This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

PDF Catalog

PDF Pages PDF Title
1 Scope
Referenced Documents
Summary of Test Method
Significance and Use
Interferences
2 Apparatus
Reagents and Materials
Sampling
TABLE 1
3 Preparation of Apparatus
Calibration and Standardization
Procedure A (by Mass)
Procedure B (by Volume)
4 Procedure C (Water Evaporator Accessory)
Quality Control Checks
Calculation
Report
Precision and Bias
5 Keywords
X1. HELPFUL HINTS FOR COULOMETRIC KARL FISCHER WATER ANALYSIS
X1.1
ASTM-D6304 2007
$40.63