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BS EN 16778:2016

$102.76

Protective gloves. The determination of Dimethylformamide in gloves

Published By Publication Date Number of Pages
BSI 2016 16
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This document specifies a test method for the determination of Dimethylformamide (DMFa – CAS N° 68-12-2) in glove materials.

NOTE

For Dimethylformamide the following abbreviations can be used: DMF, DMFa DMFo.

The test method is applicable for the following materials:

  • polyurethane (PU) materials (except elastane), PU Coated material (textile, leather), PU foam, PU blended materials;

  • adhesives;

  • all materials manufactured with a dipping process using DMFa.

PDF Catalog

PDF Pages PDF Title
4 Contents Page
5 European foreword
6 1 Scope
2 Normative references
3 Principle
4 Consumables
4.1 Reagents
Table 1 — Reagent used in analysis
4.2 Stock solutions
4.2.1 Internal standard — Stock solution (1000 mg/l)
4.2.2 Internal standard — working solution (200 mg/l)
7 4.2.3 Target compound — Stock solution (1000 mg/l)
4.2.4 Target compound — working solution (200 mg/l)
4.2.5 Extraction solution containing 20 mg/l internal standard
5 Equipment
6 Test procedure
6.1 Sampling
6.2 Conditioning
8 6.3 Preparation
Figure 1 — Cutting of the test piece
6.4 Extraction
9 6.5 Determination with GC-MS
6.5.1 Calibration
Table 2 — Preparation of calibration
6.5.2 Examples of instrumental method
6.5.2.1 Measuring method
6.5.2.2 Chromatographic conditions
10 6.5.2.3 Detection conditions
Table 3 — The SIM mode focus on the following ions
6.6 Quantification
11 6.7 Results
7 Performance of the method
8 Test report
12 Annex A (informative) Results of the interlaboratory trial
Table A.1 — Results of correlation trial
13 Bibliography
BS EN 16778:2016
$102.76