BS EN 196-11:2018:2019 Edition
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Methods of testing cement – Heat of hydration. Isothermal Conduction Calorimetry method
Published By | Publication Date | Number of Pages |
BSI | 2019 | 20 |
This document specifies the apparatus and procedure for determining the heat of hydration of cements and other hydraulic binders at different test ages by isothermal conduction calorimetry. This test procedure is intended for measuring the heat of hydration of cement up to 7 days in order to obtain correspondence between Isothermal Conduction Calorimetry (ICC) and EN 196 8 and EN 196 9. Nevertheless this test duration may be critical for some apparatus, even if they can work properly at shorter test ages. Contrary to EN 196 8 this method gives the heat of hydration continuously over the time. Additionally, the heat flow versus time is given.
PDF Catalog
PDF Pages | PDF Title |
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2 | National foreword |
5 | European foreword |
6 | 1 Scope 2 Normative references 3 Terms and definitions |
8 | 4 Apparatus 4.1 General 4.2 Principle |
9 | 4.3 Thermostat 4.4 Calorimeter technical parameters |
10 | 5 Calibration 5.1 General |
11 | 5.2 Steady-state calibration 5.2.1 General 5.2.2 Calibration coefficient ε |
12 | 5.2.3 Time constant τ 5.3 Pulse calibration 5.3.1 General |
13 | 5.3.2 Time constant τ |
14 | 5.4 Determination of the calorimeter parameters 5.5 Improvement of common calibration procedure 6 Sample 6.1 General 6.2 Test sample 6.3 Reference sample |
15 | 7 Testing procedure 7.1 General 7.2 Method A — “External mixing” |
16 | 7.3 Method B — “Internal mixing” 7.4 Measurement 7.5 Expression of results |
17 | 7.6 Test result |
18 | 7.7 Test report 8 Precision 8.1 Repeatability 8.2 Reproducibility |