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BS ISO 22278:2020

$167.15

Fine ceramics (advanced ceramics, advanced technical ceramics). Test method for crystalline quality of single-crystal thin film (wafer) using XRD method with parallel X-ray beam

Published By Publication Date Number of Pages
BSI 2020 38
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This document specifies the test method for measuring the crystalline quality of single-crystal thin film (wafer) using the XRD method with parallel X-ray beam. This document is applicable to all of the single-crystal thin film (wafer) as bulk or epitaxial layer structure.

PDF Catalog

PDF Pages PDF Title
2 National foreword
6 Foreword
7 Introduction
9 1 Scope
2 Normative references
3 Terms and definitions
11 4 Fundamentals
5 Devices and instruments
5.1 Schematic diagrams
12 5.2 X-ray generator
13 5.3 X-ray mirror
5.4 Monochromator
5.5 Sample attachment
5.6 Goniometer
5.7 Detector
5.8 Instrument calibration
14 6 Preparation of sample
7 Test method and procedure
7.1 Optics alignment
7.2 Sample alignment
15 7.3 Adjusting the initial position of goniometer
7.3.1 Symmetric diffraction
17 7.3.2 Asymmetric diffraction
7.4 Microscopic position adjustment of goniometer (Φ and χ axes) and ω scan
7.4.1 Symmetric diffraction
20 7.4.2 Asymmetric diffraction
24 7.5 Crystalline quality measurement method of single-crystal wafer
7.5.1 General
7.5.2 Selecting the flat zone position of wafer
25 7.5.3 Arranging the fixed size of the square
7.5.4 Measuring the FWHM value of RC
7.5.5 Interference effect by the wafer’s curvature
7.5.6 Doped epitaxy film on a single-crystal thin film substrate
26 8 Data analysis
9 Test report
28 Annex A (informative) Example of d-spacing, 2θ, χ value (tilt angle) and relative ideal intensity of the symmetric and asymmetric diffraction on the SiC single-crystal thin film (wafer)
30 Annex B (informative) Determination of d-spacing, 2θ, χ value (tilt angle) and relative ideal intensity for the symmetric and asymmetric diffraction on the single-crystal thin film (wafer)
34 Annex C (informative) Results of interlaboratory test
36 Bibliography
BS ISO 22278:2020
$167.15