BS ISO 10810:2019
$167.15
Surface chemical analysis. X-ray photoelectron spectroscopy. Guidelines for analysis
| Published By | Publication Date | Number of Pages |
| BSI | 2019 | 42 |
This document is intended to aid the operators of X-ray photoelectron spectrometers in their analysis of typical samples. It takes the operator through the analysis from the handling of the sample and the calibration and setting-up of the spectrometer to the acquisition of wide and narrow scans and also gives advice on quantification and on preparation of the final report.
PDF Catalog
| PDF Pages | PDF Title |
|---|---|
| 2 | National foreword |
| 7 | Foreword |
| 8 | Introduction |
| 9 | 1 Scope 2 Normative references 3 Terms and definitions 4 Symbols and abbreviations |
| 10 | 5 Overview of sample analysis |
| 12 | 6 Specimen characterization 6.1 General |
| 13 | 6.2 Specimen forms 6.2.1 General 6.2.2 Single crystal 6.2.3 Adsorbed or segregated layers, films and residues |
| 14 | 6.2.4 Interfaces and multilayered samples 6.2.5 Non-porous 6.2.6 Porous 6.2.7 Powder 6.2.8 Fibres and textiles 6.2.9 Internal interface 6.3 Material types 6.3.1 General 6.3.2 Metals and alloys |
| 15 | 6.3.3 Polymers 6.3.4 Semiconductors 6.3.5 Magnetic materials 6.3.6 Ceramics 6.3.7 Catalysts 6.3.8 Glass and insulators 6.3.9 Biological 6.3.10 Nanoparticles 6.4 Handling and mounting of specimens |
| 16 | 6.5 Specimen treatments 6.5.1 General 6.5.2 Heating and cooling 6.5.3 Scraping and fracture 6.5.4 Ion bombardment for analysing thin films 6.5.5 Exposure to gases and liquids 7 Instrument characterization[8] 7.1 General |
| 17 | 7.2 Instrument checks 7.2.1 System health check[9] 7.2.2 Mechanical 7.2.3 Sample holder 7.2.4 Vacuum |
| 18 | 7.3 Instrument calibration 7.3.1 Calibration of binding energy scale |
| 19 | 7.3.2 Intensity repeatability and intensity/energy response function (IERF) |
| 20 | 7.3.3 Linearity of intensity scale test |
| 21 | 7.3.4 Lateral resolution 7.3.5 Depth resolution[21][22] |
| 24 | 7.3.6 Charge correction 7.4 Instrument set-up 7.4.1 Optimum settings |
| 25 | 7.4.2 System configuration 8 The wide-scan spectrum 8.1 Data acquisition 8.1.1 General |
| 26 | 8.1.2 Sample loading 8.1.3 Energy resolution 8.1.4 Energy range, step size and acquisition mode 8.1.5 X-ray source and conditions |
| 27 | 8.1.6 Charge correction 8.1.7 Spectrum acquisition 8.1.8 X-ray degradation 8.1.9 Thin surface layer 8.2 Data analysis 8.2.1 Calibration of the binding energy scale |
| 28 | 8.2.2 Peak table 8.2.3 Quantification |
| 29 | 8.2.4 Assessment of the composition employing the Tougaard extrinsic background[42] 8.2.5 Requirement for narrow scans 9 The narrow scan 9.1 General 9.2 Data acquisition 9.2.1 Instrument settings 9.2.2 Choice of region |
| 30 | 9.3 Data analysis 9.3.1 Element identification 9.3.2 Chemical-state identification |
| 31 | 9.3.3 Quantification |
| 34 | 10 Test report |
| 36 | Bibliography |
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BS ISO 10810:2019 – TC:2020 Edition
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