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BS ISO 5667-10:2020

BS ISO 5667-10:2020

$198.66

Water quality. Sampling – Guidance on sampling of waste water

Published By Publication Date Number of Pages
BSI 2020 54
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This document contains details on the sampling of domestic and industrial waste water, i.e. the design of sampling programmes and techniques for the collection of samples. It covers waste water in all its forms, i.e. industrial waste water, radioactive waste water, cooling water, raw and treated domestic waste water.

It deals with various sampling techniques used and the rules to be applied so as to ensure the samples are representative.

Sampling of accidental spillages is not included, although the methods described in certain cases may also be applicable to spillages.

PDF Catalog

PDF Pages PDF Title
2 National foreword
7 Foreword
9 1 Scope
2 Normative references
3 Terms and definitions
11 4 General aspects
4.1 Design of sampling programme
4.2 Sampling point selection – Representativeness
12 4.3 Frequency and time of sampling
4.3.1 Number of samples
4.3.2 Sampling time for effluent stream
13 5 Sampling at specific locations
14 5.1 Sampling from sewers, channels and manholes
5.2 Sampling from waste water treatments plants
15 5.3 Sampling from industrial sites
5.4 Sampling from cooling systems
16 6 Main types of waste water sampling
6.1 Spot sampling
6.2 Composite sampling
17 7 Waste water sampling
7.1 General aspects
7.1.1 Preparation of the sampling campaign
7.1.2 Arrival on site
18 7.2 Composite sampling for waste water quality monitoring
7.2.1 General
7.2.2 Automatic composite sampling
21 7.2.3 Manual composite sampling
7.2.4 Manual sample reconstitution
22 7.3 Spot sampling in an effluent stream
7.3.1 General
23 7.3.2 Direct sampling
7.3.3 Indirect sampling
24 7.3.4 Automatic, remote start or event-triggered sampling
7.4 Spot sampling of tanks ā€” planned discharges
25 8 Sampling equipment
8.1 General
8.2 Automatic sampler
26 8.3 Manual sampling equipment
8.3.1 General
8.3.2 Ballasted sample collector
8.3.3 Bucket, vertical water sampler
27 8.4 Tank sampling equipment
8.4.1 Mixing
8.4.2 Sampling equipment
9 Homogenization, preservation, transport and storage of samples
9.1 Homogenization of collected volume
28 9.2 Distribution of collected volume into laboratory bottles
29 9.3 Preservation and packaging of samples
9.4 Transportation and reception
9.4.1 General
9.4.2 Time
9.4.3 Temperature
30 9.5 Security and traceability of samples during storage and delivery
9.5.1 Routine samples
9.5.2 Samples which might be used for legal purposes
10 Quality assurance
10.1 Avoidance of contamination
31 10.2 Sample identification and records
10.3 Assurance and quality control
11 Reports
11.1 Analytical reports
32 11.2 Sampling protocols
12 Safety precautions
12.1 General
33 12.2 Personnel safety
12.3 Equipment safety
35 Annex A (informative) Examples of sampling from tanks
38 Annex B (informative) Advantages and disadvantages of main types of waste water sampling
40 Annex C (informative) Example of cleaning protocol ā€” Sampling equipment
42 Annex D (informative) Example of field form ā€” Waste water sampling
44 Annex E (informative) Choice of compatible materials for automatic samplers
46 Annex F (informative) Comparison of types of pumping: peristaltic pump (PP) and vacuum pump (VAP)
48 Annex G (informative) Type of distribution of collected volume into laboratory bottle
49 Annex H (informative) Quality control of sampling equipment
51 Annex I (informative) Bias and repeatability
52 Bibliography

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BS ISO 5667-10:2020
$198.66